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3,5-Dimethoxybenzyl Bromide → 1-(3,5-Dimethoxybenzyl)-5-ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Dimethoxybenzyl Bromide | HCID 1274490 | — |
| 反応物 | 6-(3,5-dimethylbenzoyl)-5-ethylpyrimidine-2,4(1H,3H)-dione | HCID 22256579 | — |
| 生成物 | 1-(3,5-Dimethoxybenzyl)-5-ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione | HCID 15957740 | 50.2% |
反応手順
5-Ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and 3,5-dimethoxybenzyl bromide were reacted by the same way with the example 1 to obtain the titled compound (212 mg, yield: 50.2%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06987114B1 |
| 出典データセット | uspto-grants-2006_01 |
| ORD ID | ord-3b55a3cb7e534acd9d660846565b6f3c |
| 出典メモ | uspto-grants-2006_01 |