9-(Chloromethyl)anthracene → 1-(9-Anthrylmethyl)-6-(3,5-dimethylbenzoyl)-5-isopropyl-pyrimidine-2,4-dione

HRID 1611346

反応式

HRID 1611346 の反応式
[CH:1]([C:4]1[C:5](=[O:21])[NH:6][C:7](=[O:20])[NH:8][C:9]=1[C:10](=[O:19])[C:11]1[CH:16]=[C:15]([CH3:17])[CH:14]=[C:13]([CH3:18])[CH:12]=1)([CH3:3])[CH3:2].Cl[CH2:23][C:24]1[C:25]2[C:30]([CH:31]=[C:32]3[C:37]=1[CH:36]=[CH:35][CH:34]=[CH:33]3)=[CH:29][CH:28]=[CH:27][CH:26]=2>>[CH:26]1[C:25]2[C:30](=[CH:31][C:32]3[C:37]([C:24]=2[CH2:23][N:8]2[C:9]([C:10](=[O:19])[C:11]4[CH:12]=[C:13]([CH3:18])[CH:14]=[C:15]([CH3:17])[CH:16]=4)=[C:4]([CH:1]([CH3:3])[CH3:2])[C:5](=[O:21])[NH:6][C:7]2=[O:20])=[CH:36][CH:35]=[CH:34][CH:33]=3)[CH:29]=[CH:28][CH:27]=1

参加物

3

反応物 2

HCID 323859-(Chloromethyl)anthraceneHCID 222565826-(3,5-Dimethyl-benzoyl)-5-isopropyl-1H-pyrimidine-2,4-dione

生成物 1

HCID 159577781-(9-Anthrylmethyl)-6-(3,5-dimethylbenzoyl)-5-isopropyl-pyrimidine-2,4-dione収率 40.3%

実験手順

5-Isopropyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and 9-chloromethyl anthracene were reacted by the same way with the example 1 to obtain the titled compound (192 mg, yield: 40.3%).

出典と根拠

ORDレコード
ord-a42ea2f0ff4d425f9a86e61d97098a60
出典データセット
uspto-grants-2006_01
特許番号
US06987114B1

関連ノート

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