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5-methyl-6,7-dihydro-1-benzothiophen-4(5H)-one → 5-Methyl-4,5,6,7-tetrahydro-1-benzothiophen-4-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-methyl-6,7-dihydro-1-benzothiophen-4(5H)-one | HCID 15411508 | — |
| 反応物 | 4,5,6,7-Tetrahydro-1-benzofuran-4-amine | HCID 18525171 | — |
| 生成物 | 5-Methyl-4,5,6,7-tetrahydro-1-benzothiophen-4-amine | HCID 20348929 | — |
反応手順
Following the procedure for the preparation of 4,5,6,7-tetrahydro-1-benzofuran-4-amine but substituting 5-methyl-6,7-dihydro-1-benzothiophen-4(5H)-one and making non-critical variations provided the title compound as a oil: 1H NMR (400 MHz, CDCl3) δ) 7.12-6.99, 4.13, 3.89, 3.51, 2.86-2.74, 2.13-1.98, 1.75, 1.65, 1.15, 1.07.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06992087B2 |
| 出典データセット | uspto-grants-2006_01 |
| ORD ID | ord-745e4ebddcb044ac969cd954e732949c |
| 出典メモ | uspto-grants-2006_01 |