6,7-Dihydro-5H-cyclopenta[b]pyridin-5-amine → cis-2-ethyl-6-methoxy-2,3-dihydro-1H-inden-1-amine
反応式
N1C=CC=C2C(N)CCC=12.[CH2:11]([CH:13]1[CH2:21][C:20]2[C:15](=[CH:16][C:17]([O:22][CH3:23])=[CH:18][CH:19]=2)[C:14]1=[N:24]O)[CH3:12]>>[CH2:11]([C@H:13]1[CH2:21][C:20]2[C:15](=[CH:16][C:17]([O:22][CH3:23])=[CH:18][CH:19]=2)[C@H:14]1[NH2:24])[CH3:12]参加物
3
実験手順
Following the procedure for the preparation of 6,7-dihydro-5H-cyclopenta[b]pyridin-5-amine but substituting 2-ethyl-6-methoxy-2,3-dihydro-1H-inden-1-one oxime and making non-critical variations provided the title compound as a oil: 1H NMR (CDCl3) δ 1.03, 1.39, 2.30, 2.63, 2.86, 3.82, 4.26, 6.77, 7.12;
出典と根拠
- ORDレコード
- ord-45cc39577be948be9e5fa7a9f592f791
- 出典データセット
- uspto-grants-2006_01
- 特許番号
- US06992087B2
反応ノート
読み込み中…