Hydrochloric Acid → HCID 67876499、化合物
反応式
[N:1]1[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][CH2:9][N:10]([CH2:12][CH2:13][C:14]([O:16]CC)=[O:15])[CH3:11])=[CH:3][CH:2]=1.[ClH:19]>>[ClH:19].[N:1]1[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][CH2:9][N:10]([CH2:12][CH2:13][C:14]([OH:16])=[O:15])[CH3:11])=[CH:3][CH:2]=1参加物
3
実験手順
The ethyl 3-{N-[3-(pyrid-4-yl)propyl]-N-methyl-amino}-propionate obtained is refluxed for 24 hours with 600 ml of 4-n hydrochloric acid. The reaction mixture is evaporated to complete dryness, and the crystalline residue formed is separated, washed with water and dried yielding 3-{N-[3-(pyrid-4-yl)propyl]-N-methyl-amino}-propionic acid hydrochloride.
後処理
- customThe reaction mixture is evaporated
- customthe crystalline residue formed
- customis separated
- washwashed with water
- customdried
出典と根拠
- ORDレコード
- ord-a68c67846b0443e08c3336629ce95621
- 出典データセット
- uspto-grants-1993_03
- 特許番号
- US05190930
反応ノート
読み込み中…