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Hydrochloric Acid → N,N-Diethyl-P-phenylenediamine dihydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | N,N-Diethyl-p-phenylenediamine | HCID 7120 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | N,N-Diethyl-P-phenylenediamine dihydrochloride | HCID 19799983 | 100% |
反応手順
N,N-diethyl-p-phenylenediamine (5 g, 30.4 mmol) was dissolved in diethyl ether (25 cm3) and hydrochloric acid (6 cm3, 10 M) was added and the mixture was concentrated to give the title compound (7.22 g, 100%) as a red/brown solid. dH (250 MHz; D2O): 7.68 (4H, m, ArH), 3.69 (4H, q, 7.32, NCH2), 1.11 (6H, t, 7.32, CH3); dC (62.9 MHz; D2O): 12.1 (CH3), 56.4 (NCH2), 126.8 (ArC), 127.6 (ArC), 135.5 (ArC), 139.1 (ArC).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07737138B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-cdcfae7f36ac4516963007566eca95a0 |
| 出典メモ | uspto-grants-2010_06 |