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Borane → 2-(3,4-Dichlorophenoxy)ethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Borane | HCID 6331 | — |
| 反応物 | (3,4-Dichlorophenoxy)acetic acid | HCID 11495 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 2-(3,4-Dichlorophenoxy)ethanol | HCID 19108692 | 91% |
反応手順
The title compound was prepared by reduction of 2-(3,4-dichlorophenoxy)acetic acid (Aldrich, 96% pure) with borane in tetrahydrofuran (Aldrich, 1M solution) using the procedure of N. M. Yoon, et al. in J. Org. Chem 38(#16) p. 2786 (1973). The yield was 91% of theory.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05192785 |
| 出典データセット | uspto-grants-1993_03 |
| ORD ID | ord-7b0e61847cba4038b8a679e3b6d599da |
| 出典メモ | uspto-grants-1993_03 |