2,6-Dichlorophenol → 2,6-Dichlorophenyl sulfamate
反応式
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[OH:9].Cl[S:11]([N:14]=C=O)(=[O:13])=[O:12]>C1(C)C=CC=CC=1>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[O:9][S:11](=[O:13])(=[O:12])[NH2:14]参加物
4
実験手順
This compound was prepared according to the procedure of Example 75 from a mixture of 16.3 g (0.10 mole) of 2,6-dichlorophenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 75 ml of toluene to obtain 17.3 g (71%) of the title compound after recrystallization from benzene, mp 114.5°-116° C.
後処理
- customThis compound was prepared
出典と根拠
- ORDレコード
- ord-f669c17f7e314cc28c0d18bb4aa78384
- 出典データセット
- uspto-grants-1993_03
- 特許番号
- US05192785
反応ノート
読み込み中…