N-Methylbenzylamine hydrochloride → HCID 19773275、化合物
反応式
[C:1]([NH:4][C:5]1[CH:14]=[CH:13][CH:12]=[C:11]2[C:6]=1[CH2:7][CH2:8][C:9](=O)[CH2:10]2)(=[O:3])[CH3:2].[ClH:16].[CH2:17]([NH:24][CH3:25])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[ClH:16].[C:1]([NH:4][C:5]1[CH:14]=[CH:13][CH:12]=[C:11]2[C:6]=1[CH2:7][CH2:8][CH:9]([N:24]([CH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[CH3:25])[CH2:10]2)(=[O:3])[CH3:2]参加物
3
実験手順
Starting from 2.03 g (0.01 mol) of 5-acetylamino-2-tetralone and 4.37 g (0.03 mol) of N-benzyl-methylaminehydrochloride the title compound is obtained analogously to Example 4.1.11 in a yield of 2.0 g (58.1% of theory) and with a melting point of 243° C. which does not change after recrystallisation from methanol/ether.
出典と根拠
- ORDレコード
- ord-2350ae0a316c4ae9bff0be0cdf5ee138
- 出典データセット
- uspto-grants-1993_03
- 特許番号
- US05196454
反応ノート
読み込み中…