Hydrochloric Acid → HCID 14822258、化合物

HRID 1614562ノート

反応式

HRID 1614562 の反応式
[ClH:1].[NH2:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][C:12]([N:14]2[CH2:18][CH2:17][S:16][CH2:15]2)=[O:13])=[CH:5][CH:4]=1>>[ClH:1].[NH2:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][CH2:11][C:12]([N:14]2[CH2:18][CH2:17][S:16][CH2:15]2)=[O:13])=[CH:7][CH:8]=1

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 14822257N-[4-(4-aminophenyl)butanoyl]thiazolidine

生成物 1

HCID 14822258HCID 14822258、化合物収率 98%

実験手順

To 5 ml of alcoholic hydrogen chloride 1 mmol of N-[4-(4-aminophenyl)butanoyl]thiazolidine was added and dissolved under heating. The mixture was stirred at room temperature for 2 hours. After the reaction, the solvent was evaporated under reduced pressure. To the residue was added anhydrous ether and precipitates thus produced were collected by filtration to obtain 0.28 g of colorless crystals of N-[4-(4-aminophenyl)butanoyl]thiazolidine hydrochloride (yield: 98%).

後処理

  1. dissolutiondissolved
  2. temperatureunder heating
  3. customAfter the reaction
  4. customthe solvent was evaporated under reduced pressure
  5. additionTo the residue was added anhydrous ether
  6. customprecipitates thus
  7. customproduced
  8. filtrationwere collected by filtration

出典と根拠

ORDレコード
ord-dd4eea7a48f64c49a0fdc4e86b926e08
出典データセット
uspto-grants-1993_03
特許番号
US05198450

反応ノート

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