化工社化工社 化学情報印刷レポート · 研究参考用
Benzoyl Peroxide → Methanone, [2-(bromomethyl)phenyl]phenyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoyl Peroxide | HCID 7187 | — |
| 反応物 | N-bromobutanimide | HCID 67184 | — |
| 反応物 | 2-Methylbenzophenone | HCID 67230 | — |
| 溶媒 | Carbon Tetrachloride | HCID 5943 | — |
| 生成物 | Methanone, [2-(bromomethyl)phenyl]phenyl- | HCID 11778133 | — |
反応手順
A mixture of 2-methylbenzophenone (9.8 g), N-bromosuccinimide (8.9 g), benzoyl peroxide (0.5 g) and carbon tetrachloride (150 ml) was refluxed for 1 hour with light irradiation. The mixture was cooled, and then filtered to remove insoluble substances. The filtrate was concentrated to afford quantitatively the above-titled compound as an oily susbstance.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05198462 |
| 出典データセット | uspto-grants-1993_03 |
| ORD ID | ord-45c80e9646024cb9882f47db98e06195 |
| 出典メモ | uspto-grants-1993_03 |