1-Aminocyclohexanecarboxylic acid → Methyl 1-aminocyclohexane-1-carboxylate hydrochloride
反応式
F[C:2]1C=C(C(N)C)C=C(F)C=1.[ClH:12].[NH2:13][C:14]1([C:19]([O:21][CH3:22])=[O:20])[CH2:18][CH2:17][CH2:16][CH2:15]1.NC1(C(O)=O)CCCCC1>>[ClH:12].[NH2:13][C:14]1([C:19]([O:21][CH3:22])=[O:20])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:2]1参加物
4
実験手順
Essentially following the procedures described in Intermediate 1 for methyl 1-aminocyclopentanecarboxylate hydrochloride, but using 1-aminocyclohexanecarboxylic acid in place of 1-aminocyclopentanecarboxylic acid, the title compound was obtained. MS: m/z=158 (M+1).
出典と根拠
- ORDレコード
- ord-8cb5bc9917154894ae223626838053a8
- 出典データセット
- uspto-grants-2014_07
- 特許番号
- US08765759B2
反応ノート
読み込み中…