Methanamine, N-methoxy-, hydrochloride (1:1) → 2-(9H-Fluoren-9-yl)-N-methoxy-N-methyl-acetamide
反応式
[CH:1]1[C:13]2[CH:12]([CH2:14][C:15](O)=[O:16])[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]=2[CH:4]=[CH:3][CH:2]=1.Cl.[CH3:19][NH:20][O:21][CH3:22]>>[CH:5]1[C:13]2[CH:12]([CH2:14][C:15]([N:20]([O:21][CH3:22])[CH3:19])=[O:16])[C:11]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[C:1]=2[CH:2]=[CH:3][CH:4]=1参加物
3
実験手順
In analogy to example 55, step 1, from fluorene-9-acetic acid (CAS RN: [6284-80-6]) and N,O-dimethylhydroxylamine hydrochloride was prepared the title compound as an off-white oil, MS (ESI+): m/z=268.1 ([M+H]+).
出典と根拠
- ORDレコード
- ord-a7deb74daa8446ff849481a1cf55acff
- 出典データセット
- uspto-grants-2014_07
- 特許番号
- US08765730B2
反応ノート
読み込み中…