Ethoxyethylamine → HCID 178467931、化合物
反応式
[CH2:1]([O:3][CH2:4][CH2:5][NH2:6])[CH3:2].S=[C:8]1[CH2:12][S:11][C:10](=[O:13])[NH:9]1>C(O)C>[CH2:1]([O:3][CH2:4][CH2:5][NH:6][C:8]1[CH2:12][S:11][C:10](=[O:13])[N:9]=1)[CH3:2]参加物
4
実験手順
To a solution of 2-ethoxyethanamine (4.07 g) in ethanol (100 mL) was added 4-thioxo-1,3-thiazolidin-2-one (4.05 g), and the mixture was stirred at room temperature overnight. The reaction mixture was concentrated, and the residue was purified by silica gel column chromatography (ethyl acetate/hexane) to give the title compound (4.90 g).
後処理
- concentrationThe reaction mixture was concentrated
- customthe residue was purified by silica gel column chromatography (ethyl acetate/hexane)
出典と根拠
- ORDレコード
- ord-cc5f7d83498a4c6a9e0b61fcef548c39
- 出典データセット
- uspto-grants-2014_07
- 特許番号
- US08772277B2
反応ノート
読み込み中…