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Hydrazine → 2,4-Dimethylbenzohydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrazine | HCID 9321 | — |
| 反応物 | Methyl 2,4-dimethylbenzoate | HCID 32031 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2,4-Dimethylbenzohydrazide | HCID 4846173 | — |
反応手順
To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08784782B2 |
| 出典データセット | uspto-grants-2014_07 |
| ORD ID | ord-0c7a3d9d10ba4e2b964212cfbbb97f70 |
| 出典メモ | uspto-grants-2014_07 |