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HRID 1625872作成日:2026年10月26日

2-Phenylthiophene → 5-Bromo-2,4-dimethyl-1-(5-phenyl-2-thienylmethyl)benzene

https://huagongshe.com/reaction/1625872

反応式

関与物質

役割名称HCID仕込み量
反応物2-PhenylthiopheneHCID 69999—
反応物5-Bromo-2,4-dimethylbenzoic acidHCID 555765—
生成物5-Bromo-2,4-dimethyl-1-(5-phenyl-2-thienylmethyl)benzeneHCID 66608954—

反応手順

The above 5-bromo-2,4-dimethylbenzoic acid and 2-phenylthiophene were treated in a manner similar to Reference Example 5 to give 5-bromo-2,4-dimethyl-1-(5-phenyl-2-thienylmethyl)benzene as colorless crystals. APCI-Mass m/Z 357/359 (M+H).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08785403B2
出典データセットuspto-grants-2014_07
ORD IDord-6888c55c752c4dd597dfcd6999041e8d
出典メモuspto-grants-2014_07