Nicotinic Acid → nicotinic acid, potassium salt

HRID 1627235

反応式

HRID 1627235 の反応式
[OH-].[K+:2].[C:3]([OH:11])(=[O:10])[C:4]1[CH:9]=[CH:8][CH:7]=[N:6][CH:5]=1>O>[C:3]([O-:11])(=[O:10])[C:4]1[CH:9]=[CH:8][CH:7]=[N:6][CH:5]=1.[K+:2]

参加物

4

反応物 2

HCID 938Nicotinic AcidHCID 14797Potassium Hydroxide

生成物 1

HCID 23668574nicotinic acid, potassium salt

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
50 °C

実験手順

To a solution of KOH (1.12 g) in 10 ml of demineralised water, Nicotinic acid was added and stirred well at 50° C. for 3 h. Water was removed in a rotavapour. The solid was dried under vacuum at 120° C. to remove final traces of water to give 3.1 g of white solid with m.pt >325° C.

後処理

  1. customWater was removed in a rotavapour
  2. customThe solid was dried under vacuum at 120° C.
  3. customto remove final traces of water

出典と根拠

ORDレコード
ord-3ae00697a9454965aab53fe4794ef412
出典データセット
uspto-grants-2014_07
特許番号
US08785529B2

関連ノート

読み込み中…