化工社化工社 化学情報印刷レポート · 研究参考用
Isobutyric Acid → 1-Methyl-4-nitrosopiperidin-4-yl isobutyrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutyric Acid | HCID 6590 | — |
| 反応物 | 1-Methylpiperidin-4-one oxime | HCID 339053 | — |
| 反応物 | HCID 178418268 | HCID 178418268 | — |
| 生成物 | 1-Methyl-4-nitrosopiperidin-4-yl isobutyrate | HCID 57954508 | — |
反応手順
1-Methyl-4-nitrosopiperidin-4-yl isobutyrate was prepared from 1-methyl-piperidin-4-one oxime, lead tetraacetate and isobutyric acid using conditions of General Method 3. 1H NMR (400MHz, chloroform-d) δ 2.82-2.94 (2H, m), 2.65 (1H, sept, 7.0 Hz), 2.36 (3H, s), 2.23-2.35 (4H, m), 1.83-1.92 (2H, m), 1.28 (3H, s), 1.27 (3H, s).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08791134B2 |
| 出典データセット | uspto-grants-2014_07 |
| ORD ID | ord-8c54031138534b43b856ac1bb27e080d |
| 出典メモ | uspto-grants-2014_07 |