Carbamate → HCID 58071782、化合物
反応式
C([O:5][C:6](=[O:25])[CH2:7][C:8]1[C:9]([CH2:23][CH3:24])=[N:10][N:11]([CH2:15][C:16]2[CH:21]=[CH:20][C:19]([NH2:22])=[CH:18][CH:17]=2)[C:12]=1[CH2:13][CH3:14])(C)(C)C.[C:26](=[O:29])([O-:28])N>>[CH2:15]([O:28][C:26]([NH:22][C:19]1[CH:18]=[CH:17][C:16]([CH2:15][N:11]2[C:12]([CH2:13][CH3:14])=[C:8]([CH2:7][C:6]([OH:5])=[O:25])[C:9]([CH2:23][CH3:24])=[N:10]2)=[CH:21][CH:20]=1)=[O:29])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1参加物
3
実験手順
Example 3.3 was prepared according to the method described for method 3.1, employing intermediate 2.1.2 instead of intermediate 1.1.3 in the carbamate formation step. The subsequent cleavage of the tert-butyl ester was performed under acidic conditions as described for example 2.1.
後処理
- customExample 3.3 was prepared
出典と根拠
- ORDレコード
- ord-078b20d745c0412dbdc1f2fd8b104d83
- 出典データセット
- uspto-grants-2014_07
- 特許番号