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Aniline → N-(3-Methoxybenzylidene)aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | 3-Methoxybenzaldehyde | HCID 11569 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | N-(3-Methoxybenzylidene)aniline | HCID 555084 | — |
反応手順
A solution of 85.4 gm. of 3-methoxybenzaldehyde, 58.7 gm. of aniline, and 185 gm. of 3A molecular sieves in 700 ml. of anhydrous ether was refluxed for 16 hours. The ether was dried (Na2SO4), filtered, and concentrated in vacuo to an oil which upon distillation provided 93.2 gm of oil. b.p. 141°-143°/0.5 Torr.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04476311 |
| 出典データセット | uspto-grants-1984_10 |
| ORD ID | ord-312d2c2fdff149489cd828aa97a97e7e |
| 出典メモ | uspto-grants-1984_10 |