2-Ethylbutyraldehyde → 3,7-Diethyl-5-azanona-3,5-diene

HRID 1632820

反応式

HRID 1632820 の反応式
[OH-].[NH4+:2].[CH2:3]([CH:5]([CH2:8][CH3:9])[CH:6]=O)[CH3:4]>>[CH2:3]([C:5](=[CH:6][N:2]=[CH:6][CH:5]([CH2:8][CH3:9])[CH2:3][CH3:4])[CH2:8][CH3:9])[CH3:4]

参加物

3

反応物 2

HCID 73592-EthylbutyraldehydeHCID 14923Ammonium Hydroxide

生成物 1

HCID 124134703,7-Diethyl-5-azanona-3,5-diene収率 76.5%

実験手順

To a sample of 250 grams of 28% ammonium hydroxide was added 215 grams of 2-ethylbutyraldehyde and the heterogeneous mixture was stirred for 18 hours at ambient temperature. The resulting organic layer was separated, and after drying, slowly distilled at atmospheric pressure to yield 148.8 grams of 3,7-diethyl-5-azanona-3,5-diene.

後処理

  1. customThe resulting organic layer was separated
  2. customafter drying
  3. distillationslowly distilled at atmospheric pressure

出典と根拠

ORDレコード
ord-a939361dc65c4703b98228c5bcdd720d
出典データセット
uspto-grants-1984_10
特許番号
US04477674

関連ノート

読み込み中…