Methylhydrazine → HCID 12582663、化合物

HRID 1633060ノート

反応式

HRID 1633060 の反応式
[C:1]([N:9]1[CH2:19][CH2:18][C:12]2[N:13]=[N:14][C:15](S)=[CH:16][C:11]=2[CH2:10]1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:20][NH:21][NH2:22]>>[C:1]([N:9]1[CH2:19][CH2:18][C:12]2[N:13]=[N:14][C:15]([N:21]([CH3:20])[NH2:22])=[CH:16][C:11]=2[CH2:10]1)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

3

反応物 2

HCID 6061MethylhydrazineHCID 178519528HCID 178519528、化合物

生成物 1

HCID 12582663HCID 12582663、化合物

実験手順

A solution of 3.4 g of 6-benzoyl-5,6,7,8-tetrahydro-3-mercaptopyrido[4,3-c]pyridazine in 40 cc of methylhydrazine is stirred at a bath temperature of 110° for 11/2 hours. The oil obtained after concentrating the mixture in a vacuum is taken up in absolute ethanol, and the calculated amount of gentisic acid is added. After standing for some time the crystalline bisgentisinate of the title compound is obtained.

後処理

  1. customThe oil obtained
  2. concentrationafter concentrating the mixture in a vacuum
  3. additionthe calculated amount of gentisic acid is added
  4. customis obtained

出典と根拠

ORDレコード
ord-791487971e9a45279de47f52ace2991f
出典データセット
uspto-grants-1984_10
特許番号
US04478837

反応ノート

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