関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Paroxetine | HCID 43815 | — |
| 反応物 | Potassium Bromide | HCID 253877 | — |
| 反応物 | Tamsulosin Hydrochloride | HCID 5362376 | — |
| 生成物 | Paroxetine Hydrochloride | HCID 62878 | — |
反応手順
The composition of the solid was tested by FTIR. A Nicolet Magna IR System 750 Fourier Transform Infrared Spectrometer controlled via Nicolet Omnic ESP® software was used to obtain the spectra. A KBr beamsplitter was used and data was collected over 4000−400 cm−1 with a resolution of 4 cm−1. An MCT-A detector, cooled with liquid nitrogen, was used. The sample compartment was under constant nitrogen purge. The aperture was set at 28, the micro velocity was 1.8988 and the gain setting was 1. The contact sampler attachment, which is a horizontal internal reflection accessory, with a trough cell, containing the ZnSe 45° ATR crystal, was used. The background spectrum was air. The spectrum was obtained by averaging 100 scans. The findings were consistent with published spectra for paroxetine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US06503927B1 |
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| 出典データセット | uspto-grants-2003_01 |
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| ORD ID | ord-7122681899ae4fe88d17f372baa3e058 |
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| 出典メモ | uspto-grants-2003_01 |
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