1-Octanol → HCID 15696565、化合物
反応式
[OH:1][CH:2]1[NH:6][C:5](=[O:7])[CH2:4][CH2:3]1.[CH2:8](O)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]>>[CH2:8]([O:1][CH:2]1[NH:6][C:5](=[O:7])[CH2:4][CH2:3]1)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]参加物
3
実験手順
7.5 g of 5-hydroxy-pyrrolidin-2-one, 10 cm3 of n-octanol and 4 g of Amberlite IR 120H are heated to 60° C. for 4 hours. After filtering, the n-octanol is eliminated by distilling under reduced pressure. 5.5 g of the expected product is obtained, m.p. 36°-38° C., crystallized from hexane.
後処理
- filtrationAfter filtering
- distillationby distilling under reduced pressure
出典と根拠
- ORDレコード
- ord-1f5cd7c854d64e72960378e2514498cf
- 出典データセット
- uspto-grants-1989_11
- 特許番号
- US04882350
反応ノート
読み込み中…