関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triolein | HCID 5497163 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Ethyl Oleate | HCID 5363269 | — |
反応手順
A mixture of ethanol and oleic acid triglyceride (ethanol: 0.1 mol, oleic acid triglyceride: 0.01 mol) was added with 0.2 g of the sulfonate-group-introduced amorphous carbon synthesized in Example 1, and the resulting mixture was maintained at 80° C. for 12 hours to produce ethyl oleate. The amount of ethyl oleate produced was quantified on a gas chromatography-mass spectrometer. The yield of ethyl oleate was 30%, and the rate of production of ethyl oleate was 10 to 100 times greater than that achieved using the same weight of each of already-existing solid strong acids (hydrated niobic acid, a polymeric solid acid “Nafion”, and a polymeric solid acid “Amberlyst-15”) as a catalyst.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US08119824B2 |
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| 出典データセット | uspto-grants-2012_02 |
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| ORD ID | ord-1fe163cf92c34de5b0bd6cd132dea6de |
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| 出典メモ | uspto-grants-2012_02 |
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