化工社化工社 化学情報印刷レポート · 研究参考用
(1,3-Dioxan-2-yl)methanol → 2-(((4-(1,3-Dioxan-2-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (1,3-Dioxan-2-yl)methanol | HCID 142350 | — |
| 反応物 | 2-(((4-((2-Methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776002 | — |
| 生成物 | 2-(((4-(1,3-Dioxan-2-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66775693 | 10% |
反応手順
The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 1,3-dioxan-2-ylmethanol obtained in the step (32b) to obtain the title compound (148 mg, total yield: 10%) as a light yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08124780B2 |
| 出典データセット | uspto-grants-2012_02 |
| ORD ID | ord-3b3295f9cbd447d5abec97debf851a36 |
| 出典メモ | uspto-grants-2012_02 |