化工社化工社 化学情報印刷レポート · 研究参考用
Ethylene Glycol → Methyl 2-methyl-1,3-dioxolane-2-butanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylene Glycol | HCID 174 | — |
| 反応物 | Methyl 5-oxohexanoate | HCID 84129 | — |
| 生成物 | Methyl 2-methyl-1,3-dioxolane-2-butanoate | HCID 3310317 | — |
反応手順
Methyl 2-methyl-I,3-dioxolane-2-butanoate (25) was prepared from methyl 5-oxohexanoate and ethylene glycol in the manner described in Example 17 above on a 28 mmol scale to yield 4.94 g (94%) of product. The product was employed immediately in the manner described in Example 26 below.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05182272 |
| 出典データセット | uspto-grants-1993_01 |
| ORD ID | ord-fcc5d31c028e442db6389d0525b1e1ea |
| 出典メモ | uspto-grants-1993_01 |