Yttrium (III) nitrate hexahydrate (1:3:6) → Yttrium nitrate lanthanum nitrate

HRID 1647371

反応式

HRID 1647371 の反応式
O.O.O.O.O.O.[N+:7]([O-:10])([O-:9])=[O:8].[Y+3:11].[N+:12]([O-:15])([O-:14])=[O:13].[N+:16]([O-:19])([O-:18])=[O:17].O.O.O.O.O.O.[N+:26]([O-:29])([O-:28])=[O:27].[La+3:30].[N+:31]([O-:34])([O-:33])=[O:32].[N+:35]([O-:38])([O-:37])=[O:36]>O>[N+:7]([O-:10])([O-:9])=[O:8].[Y+3:11].[N+:12]([O-:15])([O-:14])=[O:13].[N+:16]([O-:19])([O-:18])=[O:17].[N+:26]([O-:29])([O-:28])=[O:27].[La+3:30].[N+:31]([O-:34])([O-:33])=[O:32].[N+:35]([O-:38])([O-:37])=[O:36]

参加物

4

反応物 2

HCID 166833Yttrium (III) nitrate hexahydrate (1:3:6)HCID 16211478Lanthanum nitrate hexahydrate

生成物 1

HCID 19927084Yttrium nitrate lanthanum nitrate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Yttrium nitrate hexahydrate 3.82 g and lanthanum nitrate hexahydrate 0.997 g were dissolved in 11.5 g of water to provide an aqueous solution of yttrium nitrate-lanthanum nitrate mixture. Fifteen (15.0) g of silica gel (CARIACT-30® manufactured by Fuji Devison) was impregnated with the solution prepared as described above and dried at 120° C. in air, followed by a sequential calcination in air at 500° C. for 5 hours and in nitrogen at 500° C. for 5 hours. Thus, yttrium and lanthanum oxides as supported on the silica gel were obtain. This product was labelled Catalyst (7). This support type catalyst contained 7.5 wt % of yttrium oxide and 2.5 wt % of lanthanum oxide, and had a specific surface area of 110 m2 /g.

出典と根拠

ORDレコード
ord-d377b1af89154dbfb0a0c7f4aaa390a3
出典データセット
uspto-grants-1995_07
特許番号
US05430170

関連ノート

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