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t-Butyl (8-amino-1,2,3,4-tetrahydro-3-quinolyl)carbamate → 5-((Phenylmethyl)methylamino)-5,6-dihydro-4H-imidazo(4,5,1-ij)quinolin-2(1H)-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | t-Butyl (8-amino-1,2,3,4-tetrahydro-3-quinolyl)carbamate | HCID 19108500 | — |
| 反応物 | Diethyl ether methanol | HCID 21864698 | — |
| 生成物 | 5-((Phenylmethyl)methylamino)-5,6-dihydro-4H-imidazo(4,5,1-ij)quinolin-2(1H)-one | HCID 19919484 | — |
反応手順
This compound was prepared by following the procedure of Example 44 part B, but substituting 1,2,3,4-tetrahydro-N3 -methyl-N3 -(phenylmethyl)quinoline-3,8-diamine for t-butyl (8-amino-1,2,3,4-tetrahydro-3-quinolyl)carbamate. The bulk of the product was converted to the hydrochloride salt, mp 145°-149° C. from methanol/ether.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05436240 |
| 出典データセット | uspto-grants-1995_07 |
| ORD ID | ord-46b35582400e4af981ef697cf605d7e3 |
| 出典メモ | uspto-grants-1995_07 |