Butyric Acid → Methylthiomethyl butyrate

HRID 1648896ノート

反応式

HRID 1648896 の反応式
[C:1]([OH:6])(=[O:5])[CH2:2][CH2:3][CH3:4].[CH3:7][S:8][CH2:9]Cl.C(N(CC)CC)C>>[C:1]([O:6][CH2:7][S:8][CH3:9])(=[O:5])[CH2:2][CH2:3][CH3:4]

参加物

4

反応物 3

HCID 264Butyric AcidHCID 8471TriethylamineHCID 16916Chloromethyl methyl sulfide

生成物 1

HCID 3018539Methylthiomethyl butyrate

実験手順

This product was prepared according to the procedure described in Example 1, by reacting butyric acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 71°-73° C./12 mm Hg, n20 1.4521.

後処理

  1. customThis product was prepared

出典と根拠

ORDレコード
ord-46621d5a4dad4506858a28fffd41f5bf
出典データセット
uspto-grants-1983_11
特許番号
US04414233

反応ノート

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