Isobutyric Acid → Methylthiomethyl Isobutyrate

HRID 1648897ノート

反応式

HRID 1648897 の反応式
[C:1]([OH:6])(=[O:5])[CH:2]([CH3:4])[CH3:3].[CH3:7][S:8][CH2:9]Cl.C(N(CC)CC)C>>[C:1]([O:6][CH2:7][S:8][CH3:9])(=[O:5])[CH:2]([CH3:4])[CH3:3]

参加物

4

反応物 3

HCID 6590Isobutyric AcidHCID 8471TriethylamineHCID 16916Chloromethyl methyl sulfide

生成物 1

HCID 20481371Methylthiomethyl Isobutyrate

実験手順

This product was prepared according to the procedure described in Example 1, by reacting isobutyric acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 64° C./12 mm Hg, n20 1.4470.

後処理

  1. customThis product was prepared

出典と根拠

ORDレコード
ord-34f5b980a1af4598a6d679079034e094
出典データセット
uspto-grants-1983_11
特許番号
US04414233

反応ノート

読み込み中…