Triethylamine → (Methylsulfanyl)methyl 3-methylbutanoate

HRID 1648899ノート

反応式

HRID 1648899 の反応式
[C:1]([OH:7])(=[O:6])[CH2:2][CH:3]([CH3:5])[CH3:4].[CH3:8][S:9][CH2:10]Cl.C(N(CC)CC)C>>[C:1]([O:7][CH2:8][S:9][CH3:10])(=[O:6])[CH2:2][CH:3]([CH3:5])[CH3:4]

参加物

4

反応物 3

HCID 8471TriethylamineHCID 10430Isovaleric AcidHCID 16916Chloromethyl methyl sulfide

生成物 1

HCID 3018316(Methylsulfanyl)methyl 3-methylbutanoate

実験手順

This product was prepared according to the procedure described in Example 1, by reacting isovaleric acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 78°-79° C./12 mm Hg, n20 1.4496.

後処理

  1. customThis product was prepared

出典と根拠

ORDレコード
ord-824b123f74cd4fcda75f05f255c9913b
出典データセット
uspto-grants-1983_11
特許番号
US04414233

反応ノート

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