2-Propanol, 1,3-dichloro-, 2-carbamate → 1,3-dichloropropan-2-yl carbamate;ditridecyl (Z)-but-2-enedioate

関与物質

役割	名称	HCID	仕込み量
反応物	2-Propanol, 1,3-dichloro-, 2-carbamate	HCID 68516	—
反応物	1,1-Bis(tert-butylperoxy)cyclohexane	HCID 76359	—
反応物	2-Butenedioic acid (2Z)-, 1,4-ditridecyl ester	HCID 6437427	—
生成物	1,3-dichloropropan-2-yl carbamate;ditridecyl (Z)-but-2-enedioate	HCID 131712900	—

反応条件

温度	110 °C

反応手順

To a 500 ml resin kettle equipped with an overhead stirrer and containing 200 g of Flo Mo 36 C (ethoxylated castor oil) were added 50 g ditridecyl maleate and 6 g 1,1-bis(t-butylperoxy) cyclohexane (available from Witco Chemical Company under the tradename USP-400P). The mixture was then heated to 110° C. for 4 hours under nitrogen to yield a viscous liquid surfactant of the invention (Surfactant No. 54).

情報源と証拠

DOI	10.6084/m9.figshare.5104873.v1
特許番号	US04418158
出典データセット	uspto-grants-1983_11
ORD ID	ord-b5490c8aeee542398328e4afad8692ab
出典メモ	uspto-grants-1983_11