化工社化工社 化学情報印刷レポート · 研究参考用
2,3-Dinitrotoluene → beta-Dipropylamino-2,3-dinitrostyrene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dinitrotoluene | HCID 11761 | — |
| 反応物 | 1-tert-Butoxy-N,N,N',N'-tetrapropylmethanediamine | HCID 13771313 | — |
| 生成物 | beta-Dipropylamino-2,3-dinitrostyrene | HCID 54130656 | 85.8% |
反応手順
For two hours, 5.5 g of 2,3-dinitrotoluene is heated with 13.0 g of bisdipropylamino-tert-butoxymethane to 60° C. After cooling, the reaction mixture is freed of volatile components under a high vacuum, thus obtaining 7.6 g of β-dipropylamino-2,3-dinitrostyrene as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04925854 |
| 出典データセット | uspto-grants-1990_05 |
| ORD ID | ord-beb7c777ba3f47c29ea191bf7f02fde5 |
| 出典メモ | uspto-grants-1990_05 |