2-Imidazoline → 1H-Imidazole, 2-methyl-1-(1-methylethyl)-

HRID 1651295

反応式

HRID 1651295 の反応式
[CH:1]([N:4]1[CH2:8][CH2:7][N:6]=[C:5]1[CH3:9])([CH3:3])[CH3:2].N1CCN=C1>[Co]>[CH:1]([N:4]1[CH:8]=[CH:7][N:6]=[C:5]1[CH3:9])([CH3:3])[CH3:2]

参加物

4

反応物 2

HCID 681562-ImidazolineHCID 146929591-Isopropyl-2-methylimidazoline

生成物 1

HCID 146708161H-Imidazole, 2-methyl-1-(1-methylethyl)-収率 14%

試薬・触媒・溶媒 1

HCID 104730Cobalt触媒

実験手順

The procedure of Example 1 was followed except that 26.2 g of 1-isopropyl-2-methylimidazoline and 3.0 g of a cobalt hydrogenation catalyst was charged. GLC analysis show that a 14% yield of 1-isopropyl-2-methylimidazole was obtained with 19% conversion of imidazoline.

後処理

  1. additionwas charged

出典と根拠

ORDレコード
ord-6ade72b012ba42fd837bedb4a8163a57
出典データセット
uspto-grants-1990_05
特許番号
US04927942

関連ノート

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