関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dicyclopentadiene | HCID 6492 | — |
| 反応物 | (2R,3S,4S,5R,6R)-2-(hydroxymethyl)-6-[(E)-3-phenylprop-2-enoxy]oxane-3,4,5-triol | HCID 5280656 | — |
| 生成物 | Rosin Dicyclopentadiene | HCID 131718860 | — |
反応手順
Proportions of phenolic-modified rosin (from Example 1) and dicyclopentadiene, as indicated in Table II, were charged into a one-liter autoclave reactor. The charged autoclave was purged with nitrogen and sealed. The reaction mixture was heated to 260° C. within 60 minutes and maintained at 260° C. for six hours. The reactor then was vented carefully, and the molten resin poured into an aluminum pan and allowed to cool.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05403391 |
|---|
| 出典データセット | uspto-grants-1995_04 |
|---|
| ORD ID | ord-1e1c3b7e571045d1992897fdf2e1e6be |
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| 出典メモ | uspto-grants-1995_04 |
|---|
