HCID 15239992、化合物 → methyl 6-(N,N-dimethylamino)-3-hydroxypicolinate
反応式
C([O:8][C:9]1[C:10]([C:18]([O:20][CH3:21])=[O:19])=[N:11][C:12]([N:15]([CH3:17])[CH3:16])=[CH:13][CH:14]=1)C1C=CC=CC=1>[C].[Pd].C(OCC)(=O)C>[CH3:17][N:15]([C:12]1[N:11]=[C:10]([C:18]([O:20][CH3:21])=[O:19])[C:9]([OH:8])=[CH:14][CH:13]=1)[CH3:16]参加物
4
実験手順
2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and the mixture was hydrogenated under atmospheric pressure. After completion of the reaction, the product was filtered and concentrated to obtain crystals.
後処理
- customAfter completion of the reaction
- filtrationthe product was filtered
- concentrationconcentrated
- customto obtain crystals
出典と根拠
- ORDレコード
- ord-119bbbed187147449d212ea1efbaeb9e
- 出典データセット
- uspto-grants-1995_04
- 特許番号
- US05403816
反応ノート
読み込み中…