4-iodo-N-(3-methyl-2-pyridinyl)benzenesulfonamide → Methyl 2-hydroxy-5-[2-[4-[(3-methyl-2-pyridinylamino)sulfonyl]phenyl]ethenyl]benzoate

HRID 1653894ノート

反応式

HRID 1653894 の反応式
I[C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:11][C:12]2[C:17]([CH3:18])=[CH:16][CH:15]=[CH:14][N:13]=2)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH:19]([C:21]1[CH:22]=[CH:23][C:24]([OH:31])=[C:25]([CH:30]=1)[C:26]([O:28][CH3:29])=[O:27])=[CH2:20]>>[OH:31][C:24]1[CH:23]=[CH:22][C:21]([CH:19]=[CH:20][C:2]2[CH:7]=[CH:6][C:5]([S:8]([NH:11][C:12]3[C:17]([CH3:18])=[CH:16][CH:15]=[CH:14][N:13]=3)(=[O:10])=[O:9])=[CH:4][CH:3]=2)=[CH:30][C:25]=1[C:26]([O:28][CH3:29])=[O:27]

参加物

3

反応物 2

HCID 37926154-iodo-N-(3-methyl-2-pyridinyl)benzenesulfonamideHCID 19423384Methyl 5-ethenyl-2-hydroxybenzoate

生成物 1

HCID 54178836Methyl 2-hydroxy-5-[2-[4-[(3-methyl-2-pyridinylamino)sulfonyl]phenyl]ethenyl]benzoate収率 52%

実験手順

This compound was prepared analogously to Example 3 from 4-iodo-N-(3-methyl-2-pyridinyl)-benzenesulfonamide, prepared according to Example 2a, and methyl 5-ethenyl-2-hydroxybenzoate, prepared according to Example 3a. Yield 52%.

後処理

  1. customprepared
  2. customprepared

出典と根拠

ORDレコード
ord-41b8c4306b484c5bbc0358d02ab820f1
出典データセット
uspto-grants-1995_04
特許番号
US05403930

反応ノート

読み込み中…