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2-Butyl isothiocyanate → 1-(3-Chloro-2-methylphenyl)-4-(1-methylpropyl)thiosemicarbazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Butyl isothiocyanate | HCID 78151 | — |
| 反応物 | (3-Chloro-2-methylphenyl)hydrazine | HCID 702863 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 1-(3-Chloro-2-methylphenyl)-4-(1-methylpropyl)thiosemicarbazide | HCID 20079515 | — |
反応手順
1.44 g (10 mmole) of sec-butyl isothiocyanate were added to 1.56 g (10 mmole) of 3-chloro-2-methylphenyl hydrazine dissolved in 120 ml of toluene, and the mixture was refluxed for 2 hours and then evaporated. The remanence was stirred with a small amount of hexane, separated by filtration and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05405857 |
| 出典データセット | uspto-grants-1995_04 |
| ORD ID | ord-9f0ca789e649440ebae0831a8fd3777f |
| 出典メモ | uspto-grants-1995_04 |