Indole → HCID 19791527、化合物
反応式
Cl.[CH:2]12[NH:10][CH:6]([CH2:7][CH2:8][CH2:9]1)[CH2:5][C:4](=O)[CH2:3]2.[F:12]C1C=CC(NN)=CC=1.[NH:21]1[C:29]2[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=2)C=C1>C(Cl)Cl>[F:12][N:21]1[C:29]2[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=2)[C:3]2[CH:2]3[NH:10][CH:6]([CH2:5][C:4]1=2)[CH2:7][CH2:8][CH2:9]3参加物
5
実験手順
This compound was prepared from 9-azabicyclo[3.3.1]nonan-3-one hydrochloride and 4-fluorophenylhydrazine by the Fischer indole synthesis as described in Example 1, Method A. The product was obtained as yellow crystals (74% yield), mp 200°-201° C. (from methylene chloride).
出典と根拠
- ORDレコード
- ord-54fda50e2a9a46aab7bda45e782e2c64
- 出典データセット
- uspto-grants-1993_10
- 特許番号
- US05250537
反応ノート
読み込み中…