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1,2-Diamino-3,5-bis(trifluoromethyl)benzene → N-[5,7-Bis(trifluoromethyl)benzimidazol-2-yl]-1,2,3,4-tetrahydro-1-naphthylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Diamino-3,5-bis(trifluoromethyl)benzene | HCID 2773214 | — |
| 反応物 | 1-Isothiocyanato-1,2,3,4-tetrahydronaphthalene | HCID 21393478 | — |
| 生成物 | N-[5,7-Bis(trifluoromethyl)benzimidazol-2-yl]-1,2,3,4-tetrahydro-1-naphthylamine | HCID 11603683 | — |
反応手順
The title compound was prepared from 3,5-bis(trifluoromethyl)-1,2-diaminobenzene and 1-isothiocyanato-1,2,3,4-tetrahydronaphthalene by Procedure D. The title compound was isolated by column chromatography as the free base and as a mixture of enantiomers (solid, dec. >240° C.). MS(ES+) m/z 400 ([M+1]+, 100).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07737167B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-eed1159a40e24904984eac4e15d275ed |
| 出典メモ | uspto-grants-2010_06 |