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4,5-Dimethyl-1,2-phenylenediamine → (R)-N-(5,6-Dimethylbenzimidazol-2-yl)-1,2,3,4-tetrahydro-1-naphthylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4,5-Dimethyl-1,2-phenylenediamine | HCID 76635 | — |
| 反応物 | (R)-1-isothiocyanato-1,2,3,4-tetrahydronaphthalene | HCID 24946216 | — |
| 生成物 | (R)-N-(5,6-Dimethylbenzimidazol-2-yl)-1,2,3,4-tetrahydro-1-naphthylamine | HCID 11652226 | — |
反応手順
The title compound was prepared from 4,5-dimethylphenylenediamine and (R)-l-isothiocyanato-1,2,3,4-tetrahydronaphthalene by Procedure D. The title compound was isolated by column chromatography as the free base (solid, mp 121-124° C.). MS(ES+) m/z 292 ([M+1]+, 100).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07737167B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-dad6b99b1e534901ae53ca3c06261cc2 |
| 出典メモ | uspto-grants-2010_06 |