Sulfuric Acid → 2-Methyl-1,1,1,3-tetrafluoro-2-propanol
反応式
[CH3:1][CH:2]([CH2:7][F:8])[C:3]([F:6])([F:5])[F:4].S(=O)(=O)(O)[OH:10]>O>[CH3:1][C:2]([OH:10])([CH2:7][F:8])[C:3]([F:6])([F:5])[F:4]参加物
4
実験手順
As another example, 2-methyl-1,1,1,3-tetrafluoro-2-propanol may be prepared by reacting commercially available methacrylic acid with hydrogen fluoride to form 2-methyl-3-fluoropropanoic acid which may then be fluorinated to form 2-methyl-1,1,1,3-tetrafluoropropane. The 2-methyl-1,1,1,3-tetrafluoropropane may then be dehydrogenated and reacted with sulfuric acid and then water to form 2-methyl-1,1,1,3-tetrafluoro-2-propanol.
出典と根拠
- ORDレコード
- ord-45450f49defa412ea1c2c77563c5373f
- 出典データセット
- uspto-grants-1993_10
- 特許番号
- US05254755
反応ノート
読み込み中…