2-Nonen-1-ol, (2Z)- → (Z)-non-2-enal
反応式
[CH2:1]([OH:10])/[CH:2]=[CH:3]\[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]>CCOCC.[O-2].[O-2].[Mn+4]>[CH:1](=[O:10])/[CH:2]=[CH:3]\[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]参加物
4
実験手順
Cis-2-nonenol (5 g, mole) is stirred with manganese dioxide (50 g, mole) in ether (250 ml) at room temperature for 1 hour. The mixture is filtered, ether removed, and the residue distilled to give cis-2-nonenal.
後処理
- filtrationThe mixture is filtered
- customether removed
- distillationthe residue distilled
出典と根拠
- ORDレコード
- ord-adf1a6b11a3f4f42be911cb5a07f60ed
- 出典データセット
- uspto-grants-1976_06
- 特許番号
- US03962321
反応ノート
読み込み中…