Aniline → 2-Phenylamino-N-(2-methyl-4-sulphamoylphenyl)-acetamide

HRID 1658209ノート

反応式

HRID 1658209 の反応式
Cl[CH2:2][C:3]([NH:5][C:6]1[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:8][C:7]=1[CH3:16])=[O:4].[NH2:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:18]1([NH:17][CH2:2][C:3]([NH:5][C:6]2[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:8][C:7]=2[CH3:16])=[O:4])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

参加物

3

反応物 2

HCID 6115AnilineHCID 215288492-Chloro-N-(2-methyl-4-sulphamoylphenyl)-acetamide

生成物 1

HCID 215288562-Phenylamino-N-(2-methyl-4-sulphamoylphenyl)-acetamide収率 44%

実験手順

2-Chloro-N-(2-methyl-4-sulphamoylphenyl)-acetamide (13.1g) and aniline (9.5 g) were heated together 21/2 hr on a water bath at 90°. The mixture was worked up as in Example 1(b) to yield 7 g beige crystals, m.p. 195°-196°

出典と根拠

ORDレコード
ord-a25644f5dae245b39611f5eb2fbb0219
出典データセット
uspto-grants-1976_06
特許番号
US03963706

反応ノート

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