Hydrochloric Acid → 2-methoxy-N-methyl-2-(2-pyridyl)thioacetamide hydrochloride

HRID 1659126ノート

反応式

HRID 1659126 の反応式
[CH3:1][O:2][CH:3]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][N:9]=1)[C:4]([NH:6][CH3:7])=[S:5].[ClH:14]>CCOCC>[ClH:14].[CH3:1][O:2][CH:3]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][N:9]=1)[C:4]([NH:6][CH3:7])=[S:5]

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 15581955alpha-methoxy-N-methyl-2-pyridylthioacetamide

生成物 1

HCID 214868942-methoxy-N-methyl-2-(2-pyridyl)thioacetamide hydrochloride

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

2-Methoxy-N-methyl-2-(2-pyridyl)thioacetamide (500 mg.) in ether is added to ethereal hydrogen chloride. The resulting precipitate is filtered off and recrystallized from ethanol/ether to give 2-methoxy -N-methyl-2-(2-pyridyl)thioacetamide hydrochloride.

後処理

  1. filtrationThe resulting precipitate is filtered off
  2. customrecrystallized from ethanol/ether

出典と根拠

ORDレコード
ord-127840f35e5846239719a8259a75b71f
出典データセット
uspto-grants-1976_06
特許番号
US03966945

反応ノート

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