Acrylamide → HCID 86738175、化合物
反応式
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([N:9]([CH2:18][CH:19]=[CH2:20])[CH:10]=[CH:11][CH:12]=[C:13]([C:16]#[N:17])[C:14]#[N:15])[CH:7]=[CH2:8]>C(O)C>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:6]([N:9]([CH:10]=[CH:11][CH:12]=[C:13]([C:14]#[N:15])[C:16]#[N:17])[CH2:18][CH:19]=[CH2:20])[CH:7]=[CH2:8]参加物
4
実験手順
A solution of 40 g. of acrylamide, 52 g. of 3-diallylaminoallylidenemalononitrile (A) in 900 cc. of ethanol was refluxed. 1.3 g. of AZBN was added and the solution refluxed for two hours. At two hour time intervals, the following solutions were added in this order by refluxing:
後処理
- additionof AZBN was added
- temperaturethe solution refluxed for two hours
- additionthe following solutions were added in this order
- temperatureby refluxing
出典と根拠
- ORDレコード
- ord-a20e085380b54c7fbce2344106db85a8
- 出典データセット
- uspto-grants-1981_12
- 特許番号
- US04307184
反応ノート
読み込み中…