N-Hydroxyphthalimide → O-(2-cyclopentylethyl)hydroxylamine

反応式

O[N:2]1C(=O)C2=CC=CC=C2C1=O.[CH:13]1([CH2:18][CH2:19][OH:20])[CH2:17][CH2:16][CH2:15][CH2:14]1>>[CH:13]1([CH2:18][CH2:19][O:20][NH2:2])[CH2:17][CH2:16][CH2:15][CH2:14]1

参加物

反応物 2

HCID 10665N-Hydroxyphthalimide

HCID 69833Cyclopentaneethanol

生成物 1

HCID 21414855O-(2-cyclopentylethyl)hydroxylamine

実験手順

Prepared by a similar procedure as described for preparation 31. Starting materials: N-hydroxyphthalimide and 2-cyclopentylethanol (Lancaster). 13C-NMR (CDCl3) δ 75.7, 37.0, 34.6, 32.8, 25.1.

後処理

customPrepared by a similar procedure
customas described for preparation 31

出典と根拠

ORDレコード: ord-774195c1bd814ea28313c0b0e90d6b08
出典データセット: uspto-grants-2011_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08034811B2

反応ノート

読み込み中…