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HRID 1665862作成日:2026年10月26日

Methacrolein → 1-Acetoxy-2-Methyl-3-(3,4-Methylenedioxyphenyl)Propene

https://huagongshe.com/reaction/1665862

反応式

関与物質

役割名称HCID仕込み量
反応物MethacroleinHCID 6562—
反応物Acetic AnhydrideHCID 7918—
反応物3-(3,4-Methylenedioxyphenyl)-2-methylpropanalHCID 64805—
生成物1-Acetoxy-2-Methyl-3-(3,4-Methylenedioxyphenyl)PropeneHCID 67439826—

反応手順

The production process (B) comprises the step (3) of reacting 1,2-methylenedioxybenzene [formula (1)], methacrolein and acetic anhydride with each other to produce 1-acetoxy-2-methyl-3-(3,4-methylenedioxyphenyl)-1-propene [formula (3)]; and the step (2) of subjecting the obtained 1-acetoxy-2-methyl-3-(3,4-methylenedioxyphenyl)-1-propene [formula (3)] to hydrolysis reaction or to transesterification reaction with an alcohol, followed by subjecting the resulting reaction mixture to distillative purification.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08039649B2
出典データセットuspto-grants-2011_10
ORD IDord-360d40aed5004804bba5a3854a227e41
出典メモuspto-grants-2011_10