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2-Bromo-1-(4-bromo-2-methylphenyl)propan-1-one → 2-Bromo-1-(2-chloro-4-[1,2,4]triazol-1-yl-phenyl)-butan-1-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromo-1-(4-bromo-2-methylphenyl)propan-1-one | HCID 18520183 | — |
| 反応物 | 2-Chloro-4-(1H-1,2,4-triazol-1-yl)-benzenecarboxylic acid | HCID 18795027 | — |
| 反応物 | HCID 178418443 | HCID 178418443 | — |
| 生成物 | 2-Bromo-1-(2-chloro-4-[1,2,4]triazol-1-yl-phenyl)-butan-1-one | HCID 86638942 | — |
反応手順
This compound is prepared from 2-chloro-4-[1,2,4]triazol-1-yl-benzoic acid analgously to 2-bromo-1-(4-bromo-2-methyl-phenyl)-propan-1-one (Intermediate MA) by replacing ethylmagnesium bromide with the appropriate alkyl magnesium bromide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07994203B2 |
| 出典データセット | uspto-grants-2011_08 |
| ORD ID | ord-6ab47deff1b24250acf9d92a02d111fe |
| 出典メモ | uspto-grants-2011_08 |